退火温度对冷轧7Mn钢拉伸行为的影响及模拟研究
作者简介 阳 锋,男,1983年生,博士生
收稿日期: 2017-07-25
网络出版日期: 2017-10-19
基金资助
国家自然科学基金项目No.U1460203
Effects of Intercritical Annealing Temperature on the Tensile Behavior of Cold Rolled 7Mn Steel and the Constitutive Modeling
Received date: 2017-07-25
Online published: 2017-10-19
Supported by
Supported by National Natural Science Foundation of China (No.U1460203)
利用EBSD、TEM和XRD等手段研究了退火温度对冷轧中锰钢7%Mn-0.3%C-2%Al (质量分数)组织和力学性能的影响,并借助具物理冶金意义的本构模型探讨了冷轧中锰钢退火后的拉伸和加工硬化行为。实验结果表明,随着退火温度的上升,逆转变奥氏体的机械稳定性逐渐降低,使得应变诱导马氏体的转变速率快速上升。在700 ℃退火时,逆转变奥氏体的稳定性适中,此时材料的综合力学性能最优。模拟结果表明,奥氏体稳定性对材料的拉伸行为有决定性的影响。退火温度偏低则奥氏体稳定性过高,材料的加工硬化率和均匀延伸率都较低;若退火温度适中则奥氏体稳定性也适中,变形时能持续地产生TRIP效应硬化基体,使材料的加工硬化率和均匀延伸率均较高;退火温度偏高会导致奥氏体稳定性过低,应变诱导马氏体会在短期内大量形成,致使材料的抗拉强度较高但均匀延伸率降低。
阳锋 , 罗海文 , 董瀚 . 退火温度对冷轧7Mn钢拉伸行为的影响及模拟研究[J]. 金属学报, 2018 , 54(6) : 859 -867 . DOI: 10.11900/0412.1961.2017.00315
Medium Mn steel is composed of sub-micron grained ferrite and austenite, the unstable austenite may transform to martensite during plastic straining. Although the mechanical properties of medium Mn steel could be easily tested by tensile test, it is quite difficult to directly measure the influences of different constituent phases on the tensile and work hardening behavior. Thus, at the present work, EBSD, TEM, XRD and a constitutive model based on dislocation density have been used to study the effects of intercritical annealing (IA) temperature on the tensile properties and work hardening behavior of a newly designed medium Mn steel, Fe-7%Mn-0.3%C-2%Al (mass fraction). Experimental results showed that with the increase of IA temperature, the mechanic stability of reverted austenite decreased gradually and the kinetics of strain induced martensite rose rapidly. The stability of the reverted austenite was moderate when intercritically annealed at 700 ℃, this led to the best plasticity and the optimal mechanical properties. Simulated results exhibited that the mechanic stability of austenite has a decisive influence on the tensile behavior of the material. The austenite stability will be too high if the IA temperature is lower, and this will lead to the lower work hardening rate and uniform elongation; when the IA temperature is moderate, the stability of austenite will be optimum, consequently strain-induced martensite would be progressively produced during straining and result in the higher work hardening rate and prolonged uniform elongation; the stability of austenite will be too lower if the IA temperature is higher, thus larger volume fraction of strain-induced martensite would be formed in a short period, and this would result in the higher tensile strength but the inferior uniform elongation.
Key words: medium Mn steel; austenite stability; TRIP effect
| [1] | Heimbuch R. Overview: Auto/steel partnership [EB/OL]. |
| [2] | Cao W Q, Wang C, Shi J, et al.Microstructure and mechanical properties of Fe-0.2C-5Mn steel processed by ART-annealing[J]. Mater. Sci. Eng., 2011, A528: 6661 |
| [3] | Shi J, Sun X J, Wang M Q, et al.Enhanced work-hardening behavior and mechanical properties in ultrafine-grained steels with large-fractioned metastable austenite[J]. Scr. Mater., 2010, 63: 815 |
| [4] | Luo H W, Shi J, Wang C, et al.Experimental and numerical analysis on formation of stable austenite during the intercritical annealing of 5Mn steel[J]. Acta Mater., 2011, 59: 4002 |
| [5] | Lee S, Estrin Y, De Cooman B C. Constitutive modeling of the mechanical properties of V-added medium manganese TRIP steel[J]. Metall. Mater. Trans., 2013, 44A: 3136 |
| [6] | Suh D W, Park S J, Lee T H, et al.Influence of Al on the microstructural evolution and mechanical behavior of low-carbon, manganese transformation-induced-plasticity steel[J]. Metall. Mater. Trans., 2010, 41A: 397 |
| [7] | Lee S, De Cooman B C. Tensile behavior of intercritically annealed 10 pct Mn multi-phase steel[J]. Metall. Mater. Trans., 2014, 45A: 709 |
| [8] | Lee S, De Cooman B C.Effect of the intercritical annealing temperature on the mechanical properties of 10 Pct Mn multi-phase steel[J]. Metall. Mater. Trans., 2014, 45A: 5009 |
| [9] | Cai Z H, Ding H, Misra R D K, et al. Austenite stability and deformation behavior in a cold-rolled transformation-induced plasticity steel with medium manganese content[J]. Acta Mater., 2015, 84: 229 |
| [10] | Park S J, Hwang B, Lee K H, et al.Microstructure and tensile behavior of duplex low density steel containing 5 mass% aluminum[J]. Scr. Mater., 2013, 68: 365 |
| [11] | Yang F, Luo H W, Hu C D, et al.Effects of intercritical annealing process on microstructures and tensile properties of cold-rolled 7Mn steel[J]. Mater. Sci. Eng., 2017, A685: 115 |
| [12] | Sun C Y, Huang J, Guo N, et al.A physical constitutive model for Fe-22Mn-0.6C TWIP steel based on dislocation density[J]. Acta Metall. Sin., 2014, 50: 1115(孙朝阳, 黄杰, 郭宁等. 基于位错密度的Fe-22Mn-0.6C型TWIP钢物理本构模型研究[J]. 金属学报, 2014, 50: 1115) |
| [13] | Li Z, Wu D.Effects of hot deformation and subsequent austempering on the mechanical properties of Si-Mn TRIP steels[J]. ISIJ Int., 2006, 46: 121 |
| [14] | Ungár T, Borbély A.The effect of dislocation contrast on X-ray line broadening: A new approach to line profile analysis[J]. Appl. Phys. Lett., 1996, 69: 3173 |
| [15] | Ungár T, Dragomir I, Révész á, et al.The contrast factors of dislocations in cubic crystals: The dislocation model of strain anisotropy in practice[J]. J. Appl. Cryst., 1999, 32: 992 |
| [16] | Yang F, Luo H W, Zhang S L, et al.On the characteristics of Portevin-Le Chatelier bands in cold-rolled 7Mn steel showing transformation-induced plasticity[J]. Int. J. Plast., 2018, 103: 188 |
| [17] | Han J, Lee S J, Jung J G, et al.The effects of the initial martensite microstructure on the microstructure and tensile properties of intercritically annealed Fe-9Mn-0.05C steel[J]. Acta Mater., 2014, 78: 369 |
| [18] | Olson G, Cohen M.Kinetics of strain-induced martensitic nucleation[J]. Metall. Trans., 1975, 6A: 791 |
| [19] | Yen H W, Ooi S W, Eizadjou M, et al.Role of stress-assisted martensite in the design of strong ultrafine-grained duplex steels[J]. Acta Mater., 2015, 82: 100 |
| [20] | Bouaziz O, Buessler P.Iso-work increment assumption for heterogeneous material behaviour modelling[J]. Adv. Eng. Mater., 2004, 6: 79 |
| [21] | Jian W W, Cheng G M, Xu W Z, et al.Physics and model of strengthening by parallel stacking faults[J]. Appl. Phys. Lett., 2013, 103: 133108 |
| [22] | Seo E J, Cho L, Estrin Y, et al.Microstructure-mechanical properties relationships for quenching and partitioning (Q&P) processed steel[J]. Acta Mater., 2016, 113: 124 |
| [23] | Liang Z Y, Wang X, Huang W, et al.Strain rate sensitivity and evolution of dislocations and twins in a twinning-induced plasticity steel[J]. Acta Mater., 2015, 88: 170 |
| [24] | Bouaziz O, Allian S, Scott C.Effect of grain and twin boundaries on the hardening mechanisms of twinning-induced plasticity steels[J]. Scr. Mater., 2008, 58: 484 |
| [25] | Mecking H, Kocks U F.Kinetics of flow and strain-hardening[J]. Acta Metall., 1981, 29: 1865 |
| [26] | Estrin Y, Mecking H.A unified phenomenological description of work hardening and creep based on one-parameter models[J]. Acta Metall., 1984, 32: 57 |
| [27] | Bouaziz O, Estrin Y, Bréchet Y, et al.Critical grain size for dislocation storage and consequences for strain hardening of nanocrystalline materials[J]. Scr. Mater., 2010, 63: 477 |
| [28] | Cheng S, Spencer J A, Milligan W W.Strength and tension/compression asymmetry in nanostructured and ultrafine-grain metals[J]. Acta Mater., 2003, 51: 4505 |
| [29] | Hazra S S, Pereloma E V, Gazder A A.Microstructure and mechanical properties after annealing of equal-channel angular pressed interstitial-free steel[J]. Acta Mater., 2011, 59: 4015 |
| [30] | Liu J, Zhu G, Mao W, et al.Modeling of critical grain size for shifting plasticity enhancement to decrease by refining grain size[J]. Mater. Sci. Eng., 2014, A607: 302 |
/
| 〈 |
|
〉 |