论文

包晶合金定向凝固过程中的对流效应及带状组织形成机制 I.实验结果

  • 骆良顺 ,
  • 张宇民 ,
  • 苏彦庆 ,
  • 王新 ,
  • 郭景杰 ,
  • 傅恒志
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  • 1. 哈尔滨工业大学材料科学与工程学院, 哈尔滨 150001
    2. 哈尔滨工业大学特种环境复合材料技术国防科技重点实验室, 哈尔滨 150001
骆良顺, 1980年生, 助理研究员, 博士

收稿日期: 2010-09-19

  修回日期: 2010-11-25

  网络出版日期: 2011-03-11

基金资助

国家自然科学基金项目50901025和50771041, 中国博士后科学基金项目20090450840以及黑龙江省博士后科学基金项目资助

CONVECTION EFFECTS AND BANDING STRUCTURE FORMATION MECHANISM DURING DIRECTIONAL SOLIDIFICATION OF PERITECTIC ALLOYS
I. Experimental Result

  • LUO Liang-Shun ,
  • ZHANG Yu-Min ,
  • SU Pan-Qiang ,
  • YU Xin ,
  • GUO Jing-Jie ,
  • FU Heng-Zhi
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  • 1. School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001
    2. National Key Laboratory of Science and Technology on Advanced Composites in Special Environment, Harbin Institute
    of Technology, Harbin 150001

Received date: 2010-09-19

  Revised date: 2010-11-25

  Online published: 2011-03-11

Supported by

Supported by National Natural Science Foundation of China (Nos.50901025 and 50771041) and National Science Foundation for Post–doctoral Scientists of China (No.20090450840)

摘要

利用电阻加热和感应加热Bridgman定向凝固系统对非小平面包晶系模型合金Fe-Ni合金进行系统的定向凝固实验研究, 探索2种常规定向凝固条件下对流对包晶合金定向凝固过程中带状组织和宏观偏析的影响规律.发现在高G/V定向凝固过程中, 对流使包晶合金定向凝固过程中轴向和径向形成严重的宏观偏析, 从而使组织演化异常复杂且难以达到稳态.轴向宏观偏析体现在有限长试样从定向凝固开始至凝固结束都将发生初生相向包晶相的转变过程, 转变过程受合金成分和对流强度影响.径向宏观偏析体现在试样心部贫溶质易形成初生相, 边缘富集溶质易形成包晶相, 在径向上也存在初生相向包晶相的转变过程.

本文引用格式

骆良顺 , 张宇民 , 苏彦庆 , 王新 , 郭景杰 , 傅恒志 . 包晶合金定向凝固过程中的对流效应及带状组织形成机制 I.实验结果[J]. 金属学报, 2011 , 47(3) : 275 -283 . DOI: 10.3724/SP.J.1037.2010.00485

Abstract

Systematic directional solidification experiments were conducted to investigate the convection effects on the banding structure evolution and macrosegregation in nonfaceted–non–faceted model Fe–Ni alloy using conventional resistance heating and induction heating Bridgman directional solidification methods in this paper. It was found that convection can induce severe axial and radial macrosegregation in the directionally solidified samples, and make the microstructures complex and mae the steady state difficult to achieve. Axiamacrosegregation was reflectein finite samples olidified from the beginning to the enof soidification with the transiion from primary phase to peritectic phase. The primary–peritectic transition depended on the alloy composition and convection strengh. Radial macrosegregation reflected in the solute concentration poor in the center and rich in edge, and a primary–peritectic transition also exist in the lateral directional from the sample to the edge.

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