利用电阻加热和感应加热Bridgman定向凝固系统对非小平面包晶系模型合金Fe-Ni合金进行系统的定向凝固实验研究, 探索2种常规定向凝固条件下对流对包晶合金定向凝固过程中带状组织和宏观偏析的影响规律.发现在高G/V定向凝固过程中, 对流使包晶合金定向凝固过程中轴向和径向形成严重的宏观偏析, 从而使组织演化异常复杂且难以达到稳态.轴向宏观偏析体现在有限长试样从定向凝固开始至凝固结束都将发生初生相向包晶相的转变过程, 转变过程受合金成分和对流强度影响.径向宏观偏析体现在试样心部贫溶质易形成初生相, 边缘富集溶质易形成包晶相, 在径向上也存在初生相向包晶相的转变过程.
Systematic directional solidification experiments were conducted to investigate the convection effects on the banding structure evolution and macrosegregation in nonfaceted–non–faceted model Fe–Ni alloy using conventional resistance heating and induction heating Bridgman directional solidification methods in this paper. It was found that convection can induce severe axial and radial macrosegregation in the directionally solidified samples, and make the microstructures complex and mae the steady state difficult to achieve. Axiamacrosegregation was reflectein finite samples olidified from the beginning to the enof soidification with the transiion from primary phase to peritectic phase. The primary–peritectic transition depended on the alloy composition and convection strengh. Radial macrosegregation reflected in the solute concentration poor in the center and rich in edge, and a primary–peritectic transition also exist in the lateral directional from the sample to the edge.
[1] Kerr H W, Kurz W. Int Mater Rev, 1996; 41: 129
[2] Johnson D R, Inui H, Yamaguchi M. Acta Mater, 1996;44: 2523
[3] Lapin J, Klimova A, Velisek R, Kursa M. Scr Mater, 1997; 37: 85
[4] Zhong H, Li S M, Lu H Y, Liu L, Zou G R, Fu H Z. J Cryst Growth, 2008; 310: 3366
[5] Li S M, Ma B L, L¨u H Y, Liu L, Fu H Z. Acta Metall Sin, 2005; 41: 411
(李双明, 马伯乐, 吕海燕, 刘林, 傅恒志. 金属学报, 2005; 41: 411)
[6] Nagashio K, Takamura Y, Kuribayashi K. Scr Mater, 1999; 41: 1161
[7] Liu Y C. PhD Thesis, Northwestern Polytechnical University, Xi’an, 2000
(刘永长. 西北工业大学博士学位论文, 西安, 2000)
[8] Wang M. PhD Thesis, Northwestern Polytechnical University, Xi’an, 2002
(王猛. 西北工业大学博士学位论文, 西安, 2002)
[9] Fu H Z, Su Y Q, Guo J J, Xu D M. Acta Metall Sin, 2002; 38: 9
(傅恒志, 苏彦庆, 郭景杰, 徐达鸣. 金属学报, 2002; 38: 9)
[10] Dobler S, Lo T S, Plapp M, Karma A, Kurz W. Acta Mater, 2004; 52: 2795
[11] Su Y Q, Luo L S, Li X Z, Guo J J, Yang H M, Fu H Z. Appl Phys Lett, 2006; 89: 031918
[12] Trivedi R. Metall Trans, 1995; 26A: 1583
[13] Liu S, Trivedi R. Metall Trans, 2006; 37A: 3293
[14] Trivedi R, Shin J H. Mater Sci Eng, 2005; A413: 288
[15] Li X Z, Guo J J, Su Y Q, Wu S P, Fu H Z. Acta Metall Sin, 2005; 41: 593
(李新中, 郭景杰, 苏彦庆, 吴士平, 傅恒志. 金属学报, 2005; 41: 593)
[16] Guo J J, Li X Z, Su Y Q, Wu S P, Fu H Z. Acta Metall Sin, 2005; 41: 599
(郭景杰, 李新中, 苏彦庆, 吴士平, 傅恒志. 金属学报, 2005; 41: 599)
[17] Li S M, Liu L, Li X L, Fu H Z. Acta Metall Sin, 2004; 40: 20
(李双明, 刘林, 李晓历, 傅恒志.金属学报, 2004; 40: 20)
[18] Luo L S. PhD Thesis, Harbin Institute of Technology, 2008
(骆良顺. 哈尔滨工业大学博士学位论文, 2008)
[19] Karma A, Rappel W J, Fuh B C, Trivedi R. Metall Trans, 1998; 29A: 1457
[20] Luo L S, Su Y Q, Guo J J, Li X Z, Yang H M, Fu H Z. Appl Phys Lett, 2008; 92: 061903
[21] Xu X. Master Dissertation, Northwestern Polytechnical University, Xi’an, 2005
(许雄. 西北工业大学硕士学位论文, 西安, 2005)