本文在540-640 ℃温度范围内, 研究了真空热压温度对15%(体积分数)SiCp/2009Al复合材料的微观组织和力学性能的影响. 复合材料的致密度随热压温度升高而增加, 在580 ℃达到最大值, 高于580 ℃时下降. TEM界面观察发现:热压温度为540和560 ℃时复合材料界面结合较弱, 界面出现开裂现象;当热压温 度为580和600 ℃时界面清洁、结合较好; 当温度高于620 ℃时,复合材料界面有MgAl2O4和Al4C3形成.复合材料的强度和塑性均在580 ℃取得最佳值. 拉伸断口观察发现:热压温度低于560 ℃时, 复合材料的断裂以界面脱黏为主;热压温度在580-600 ℃之间时, 复合材料以基体的韧性断裂和颗粒的断裂为主; 热压温度高于620 ℃时, 复合材料界面处MgAl2O4和Al4C3脆性相的形成使界面开裂, 复合材料的断裂为基体韧性断裂、界面开裂以及SiC颗粒断裂.
The effects of hot pressing temperature on microstructures and tensile properties of 15% (volume fraction) SiCp/2009Al composites were investigated in this paper. The relative density of the composites increased rapidly with increasing the hot pressing temperature up to 580 ℃ and decreased with further increasing the temperatures. TEM observations revealed that the interface bonding was quite weak with the interface crack when the hot pressing temperature was below 560 ℃. When the composites were hot pressed at 580 and 600 ℃, the interface was clean and had a good interface bonding. The MgAl2O4 and Al4C3 formed at the interfaces when the hot pressing temperature was above 620 ℃. Tensile tests indicated that the composite fabricated at 580 ℃ exhibited the optimum strengtand ductility. Fractography revealed that for the composite fabricated at the hot pessing temperture below 560 ℃, the fracture mechanism was mainly the interfacial debonding. For the compositfabrcated at 580 and 600 ℃, the fracture mechanism of the composite was the matrix ductile fracture and the SiC particle fracture, When the hot pressing temperature was above 620 ℃, the interface fractured along MgAl2O4 and Al4C3, and the fracture mechanism of the composite was the matrix ductile fracture, the interface crack and the particle fracture.
[1] Ouyang Q B, Li R X, Wang W L, Zhang G D, Zhang D. Mater Sci Forum, 2007; 546–549: 1551
[2] Chawla N. Adv Mater Process, 2006; 164(7): 29
[3] Rawal S. J Met, 2001; 53(4): 14
[4] Chawla N, Chawla K K. J Met, 2006; 58(11): 67
[5] Evans R D, Boyd J D. Scr Mater, 2003; 49: 59
[6] Zhou J, Dru˙zd˙zel A T, Duszczyk J. J Mater Sci, 1999; 34: 5089
[7] Gupta A K. Bull Mater Sci, 1995; 18: 773
[8] Geng L, Qu S J, Lei T Q. Key Eng Mater, 2003; 249: 233
[9] Savitskii A P, Romanov G N, Marisunova L S. Russ Phys J, 1968; 11(8): 5
[10] Savitskii A P, Romanov G N. Powder Metall Met Ceram, 1986; 25: 184
[11] Min K H, Kang S P, Lee B H, Lee J K, Kim Y D. J Alloys Compd, 2006; 419: 290
[12] Rahimian M, Ehsani N, Parvin N, Baharvandi H R. J Mater Process Technol, 2009; 209: 5387
[13] Hong S H, Chung K H. Mater Sci Eng, 1995; A194: 165
[14] Song M, He Y H. Mater Des, 2010; 31: 985
[15] Min K H, Kang S P, Kim D G, Kim Y D. J Alloys Compd, 2005; 400: 150
[16] Fogagnolo J B, Robert M H, Torralba J M. Mater Sci Eng, 2006; A426: 85
[17] Shin K S, Chung D S, Lee S H. Metall Mater Trans, 1997; 28A: 2625
[18] Laurent V, Chatain D, Eustathopoulos N. Mater Sci Eng, 1991; A135: 894
[19] Gu M Y, Mei Z, Jin Y P, Wu Z A. Scr Mater, 1999; 40: 985
[20] Shi Z L, Ochiai S, Hojo M, Lee J C, Gu M Y, Lee H, Wu R J. J Mater Sci, 2001; 36: 2441
[21] Luo Z P, Song Y G, Zhang S Q. Scr Mater, 2001; 45: 1183
[22] Wang N, Wang Z R, Weatherly G C. Metall Trans, 1992; 23A: 1423
[23] RatnaParkhi P L, Howe J M. Metall Mater Trans, 1994; 25A: 617
[24] Zhong W M, Esperance G L, Suery M. Metall Mater Trans, 1995; 26A: 2637
[25] Gonzalez G, Salvo L, Suery M, L’Esp´erance G. Scr Metall Mater, 1995; 33: 1969
[26] Wang N, Wang Z, Weatherly G C. Metall Trans, 1979; 23A: 1423
[27] Kim Y M, Lee J C. Mater Sci Eng, 2006; A420: 8
[28] Carotenuto G, Gallo A, Nicolais L. J Mater Sci, 1994; 29: 4967
[29] Lloyd D J, Lagaoe H, McLeod A, Morris P L. Mater Sci Eng, 1989; A107: 73
[30] Sahin Y. Mater Des, 2006; 24: 671
[31] Carim A H. Mater Lett, 1991; 12: 153
[32] Man C F, Mummery P M, Derby B, Jenkins M L. In: Frank J ed., Proc 2nd Int Conf Interfacial Phenomena in Composite Materials, Leuven: Butterworth–Heinemann,
1991: 175
[33] Thebaud F, Herve E, Silva R D, Suery M, Bretheau T. In: Frank J ed., Proc 2nd Int Conf Interfacial Phenomena in Composite Materials, Leuven: Butterworth–Heinemann,
1991: 179