利用<strong>ZrO<sub>2</sub></strong> 固体电解质研究<strong>Na<sub>3</sub>AlF<sub>6</sub>-SiO<sub>2</sub></strong> 熔盐中的电沉积

利用ZrO₂ 固体电解质研究Na₃AlF₆-SiO₂ 熔盐中的电沉积

高运明, 何林, 秦庆伟, 李光强

ZrO₂ Solid Electrolyte Aided Investigation on Electrodeposition in Na₃AlF₆-SiO₂ Melt

GAO Yunming, HE Lin, QIN Qingwei, LI Guangqiang

表3 对应于图6中各点位的EDS结果

Table 3 EDS results corresponding to the points in Fig.6

Point	Mass fraction of element / %							Possible phase
Point	(atomic fraction / %)							Possible phase
	(atomic fraction / %)
	O	Ir	Zr	Si	Al	Fe	Au
	O	Ir	Zr	Si	Al	Fe	Au
1	7.61	19.43	32.85			1.76	38.36	Fe-Ir, ZrO₂
	(40.88)	(8.69)	(30.97)			(2.71)	(16.75)
2		55.56					44.44	Ir
		(56.16)					(43.84)
3		72.67		1.31		13.22	12.79	Fe-Si-Ir
		(52.04)		(6.44)		(32.58)	(8.94)
4		48.14		1.82			50.04	Ir-Si
		(43.99)		(11.39)			(44.62)
5		48.74		2.37			48.89	Ir-Si
		(43.27)		(14.37)			(42.35)
6		42.81		6.02			51.16	Ir-Si
		(31.96)		(30.77)			(37.27)
7			44.33	11.81			43.86	Zr₅Si₄
			(43.04)	(37.24)			(19.72)
8		40.30	2.59	6.90	1.17		49.04	Si _x Al _y Zr _z Ir _m
		(27.01)	(3.66)	(31.64)	(5.61)		(32.08)
9		44.83		5.45	0.32		49.40	Si _x Al _y Ir _z
		(33.80)		(28.13)	(1.73)		(36.34)
10		39.00	6.98	6.14	0.22		47.66	Si _x Al _y Zr _z Ir _m
		(27.12)	(10.22)	(29.24)	(1.07)		(32.35)
11		44.51		5.62	0.38		49.50	Si _x Al _y Ir _z
		(33.22)		(28.70)	(2.02)		(36.05)