阳极氧化法制备Zr-17Nb合金表面氧化物纳米管阵列及其性能研究
李玲1,姚生莲1,赵晓丽2,3,杨佳佳1,王野熹1,王鲁宁1,4(
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Fabrication and Properties of Anodic Oxide Nanotubular Arrays on Zr-17Nb Alloy
Ling LI1,Shenglian YAO1,Xiaoli ZHAO2,3,Jiajia YANG1,Yexi WANG1,Luning WANG1,4()
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图7. Zr-17Nb合金、阳极氧化120 min及阳极氧化120 min并经过450 ℃退火处理制备的纳米管阵列的XPS
Fig.7. XPS survey spectra of three groups of samples (Zr-17Nb, nanotubular array prepared by anodizing for 120 min, nanotubular array prepared by anodizing for 120 min and annealing at 450 ℃) (a) and high resolution spectra of Zr3d (b), Nb3d (c), O1s (d) and F1s (e) on nanotubular array anodized for 120 min before and after annealing treatment at 450 ℃
