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| Crack Formation and Healing Mechanisms in Additively Manufactured Hard-Deformed Ni-Based Superalloy GH4975 |
YE Xianwen, YAO Zhihao( ), WANG Hongying, WANG Zicheng, ZHANG Longyao, DONG Jianxin |
| School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China |
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Cite this article:
YE Xianwen, YAO Zhihao, WANG Hongying, WANG Zicheng, ZHANG Longyao, DONG Jianxin. Crack Formation and Healing Mechanisms in Additively Manufactured Hard-Deformed Ni-Based Superalloy GH4975. Acta Metall Sin, 2025, 61(12): 1845-1857.
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Abstract Ni-based superalloys that are difficult to deform are highly susceptible to cracking during additive manufacturing. Despite their importance, limited research has been conducted on the additive manufacturing of GH4975 superalloy. To address the cracking issues associated with such superalloys, this study focuses on additively manufactured GH4975 superalloy to investigates various crack repair strategies. Experimental approaches, including the addition of TiC heterogeneous nucleating agents to the powder, hot isostatic pressing (HIP), and hot compression, were used to explore effective methods and underlying mechanisms for crack healing. The results show that the calculated mismatch of close-packed planes between TiC and the matrix is 6.0%, with an atomic mismatch of 0.4% in the close-packed direction. Following the addition of nano-TiC particles, the average grain diameter of the GH4975 superalloy decreased from 41.9 μm to 27.2 μm, indicating significant grain refinement; however, the cracks were not effectively eliminated. The HIP repair method further removed some cracks, but microcracks wider than 3 μm remained unhealed. The most effective crack elimination was achieved through hot compression at 1200 °C with a strain rate of 0.1 s-1 and 30% deformation, which nearly eliminated cracks at the center of the as-printed sample. However, the crack healing ability decreased when hot compression was applied to samples that had already undergone HIP treatment. The main mechanisms of crack healing were identified as matrix plastic flow under external pressure and the diffusion-driven crack filling by Al elements.
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Received: 14 June 2024
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| Fund: National Natural Science Foundation of China(52271087) |
Corresponding Authors:
YAO Zhihao, professor, Tel: (010)62332884, E-mail: zhihaoyao@ustb.edu.cn
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| [1] |
Mostafaei A, Ghiaasiaan R, Ho I T, et al. Additive manufacturing of nickel-based superalloys: A state-of-the-art review on process-structure-defect-property relationship [J]. Prog. Mater. Sci., 2023, 136: 101108
|
| [2] |
Singh V K, Sahoo D, Amirthalingam M, et al. Dissolution of the laves phase and δ-precipitate formation mechanism in additively manufactured Inconel 718 during post printing heat treatments [J]. Addit. Manuf., 2024, 81: 104021
|
| [3] |
Pleass C, Jothi S, Krishnan M. Grain boundary and triple junction characteristics analytics of additive manufactured Inconel 625 superalloy using selective laser melting [J]. Mater. Sci. Eng., 2023, A869: 144744
|
| [4] |
Lim B, Chen H S, Chen Z B, et al. Microstructure-property gradients in Ni-based superalloy (Inconel 738) additively manufactured via electron beam powder bed fusion [J]. Addit. Manuf., 2021, 46: 102121
|
| [5] |
Kumar B, Sahu S, Srinivasan D, et al. Influence of heat input on solidification cracking in additively manufactured CM247LC Ni-based superalloy [J]. Metall. Mater. Trans., 2023, 54A: 2394
|
| [6] |
Li C, White R, Fang X Y, et al. Microstructure evolution characteristics of Inconel 625 alloy from selective laser melting to heat treatment [J]. Mater. Sci. Eng., 2017, A705: 20
|
| [7] |
Amato K N, Gaytan S M, Murr L E, et al. Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting [J]. Acta Mater., 2012, 60: 2229
|
| [8] |
Yu H, Liang J J, Bi Z N, et al. Computational design of novel Ni superalloys with low crack susceptibility for additive manufacturing [J]. Metall. Mater. Trans., 2022, 53A: 1945
|
| [9] |
Xiang X M, Jiang H, Dong J X, et al. As-cast microstructure characteristic and homogenization of a newly developed hard-deformed Ni-based superalloy GH4975 [J]. Acta Metall. Sin., 2020, 56: 988
|
|
向雪梅, 江 河, 董建新 等. 难变形高温合金GH4975的铸态组织及均匀化 [J]. 金属学报, 2020, 56: 988
|
| [10] |
van Belle L, Vansteenkiste G, Boyer J C. Investigation of residual stresses induced during the selective laser melting process [J]. Key Eng. Mater., 2013, 554-557: 1828
|
| [11] |
Kontis P, Chauvet E, Peng Z R, et al. Atomic-scale grain boundary engineering to overcome hot-cracking in additively-manufactured superalloys [J]. Acta Mater., 2019, 177: 209
|
| [12] |
Wang H, Zhang X, Wang G B, et al. Selective laser melting of the hard-to-weld IN738LC superalloy: Efforts to mitigate defects and the resultant microstructural and mechanical properties [J]. J. Alloys Compd., 2019, 807: 151662
|
| [13] |
Catchpole-Smith S, Aboulkhair N, Parry L, et al. Fractal scan strategies for selective laser melting of ‘unweldable’ nickel superalloys [J]. Addit. Manuf., 2017, 15: 113
|
| [14] |
Marchese G, Bassini E, Aversa A, et al. Microstructural evolution of post-processed Hastelloy X alloy fabricated by laser powder bed fusion [J]. Materials, 2019, 12: 486
|
| [15] |
Tomus D, Rometsch P A, Heilmaier M, et al. Effect of minor alloying elements on crack-formation characteristics of Hastelloy-X manufactured by selective laser melting [J]. Addit. Manuf., 2017, 16: 65
|
| [16] |
Engeli R, Etter T, Hövel S, et al. Processability of different IN738LC powder batches by selective laser melting [J]. J. Mater. Process. Technol., 2016, 229: 484
|
| [17] |
Zhao X M, Lin X, Chen J, et al. The effect of hot isostatic pressing on crack healing, microstructure, mechanical properties of Rene88DT superalloy prepared by laser solid forming [J]. Mater. Sci. Eng., 2009, A504: 129
|
| [18] |
Han Q Q, Mertens R, Montero-Sistiaga M L, et al. Laser powder bed fusion of Hastelloy X: Effects of hot isostatic pressing and the hot cracking mechanism [J]. Mater. Sci. Eng., 2018, A732: 228
|
| [19] |
Vilanova M, Garciandia F, Sainz S, et al. The limit of hot isostatic pressing for healing cracks present in an additively manufactured nickel superalloy [J]. J. Mater. Process. Technol., 2022, 300: 117398
|
| [20] |
Fan Z J, Li C, Yang H L, et al. Effects of TiC nanoparticle inoculation on the hot-tearing cracks and grain refinement of additively-manufactured AA2024 Al alloys [J]. J. Mater. Res. Technol., 2022, 19: 194
|
| [21] |
Zhou W Z, Zhu G L, Wang R, et al. Inhibition of cracking by grain boundary modification in a non-weldable nickel-based superalloy processed by laser powder bed fusion [J]. Mater. Sci. Eng., 2020, A791: 139745
|
| [22] |
Zhou Z P, Huang L, Shang Y J, et al. Causes analysis on cracks in nickel-based single crystal superalloy fabricated by laser powder deposition additive manufacturing [J]. Mater. Des., 2018, 160: 1238
|
| [23] |
Prasad A, Yuan L, Lee P, et al. Towards understanding grain nucleation under additive manufacturing solidification conditions [J]. Acta Mater., 2020, 195: 392
|
| [24] |
Zhou W Z, Tian Y S, Wei D Y, et al. Effects of heat treatments on the microstructure and tensile properties of IN738 superalloy with high carbon content fabricated via laser powder bed fusion [J]. J. Alloys Compd., 2023, 953: 170110
|
| [25] |
Stjohn D H, Qian M, Easton M A, et al. The interdependence theory: The relationship between grain formation and nucleant selection [J]. Acta Mater., 2011, 59: 4907
|
| [26] |
Zhang M X, Kelly P M. Edge-to-edge matching model for predicting orientation relationships and habit planes—The improvements [J]. Scr. Mater., 2005, 52: 963
|
| [27] |
Li T T. Effects and mechanisms of in-situ nanocrystals in the melt on the solidification behavior, microstructure and mechanical properties of aluminum alloys [D]. Changchun: Jilin University, 2021
|
|
李涛涛. 熔体中原位纳米晶对铝合金凝固行为、组织和力学性能影响及机制 [D]. 长春: 吉林大学, 2021
|
| [28] |
Martin J H, Yahata B D, Hundley J M, et al. 3D printing of high-strength aluminium alloys [J]. Nature, 2017, 549: 365
|
| [29] |
Wei B, Liu Z M, Cao B, et al. Cracking inhibition of nano-TiC reinforced René 104 superalloy fabricated by selective laser melting [J]. J. Alloys Compd., 2021, 881: 160413
|
| [30] |
Zheng X G, Shi Y N, Lou L H. Healing process of casting pores in a Ni-based superalloy by hot isostatic pressing [J]. J. Mater. Sci. Technol., 2015, 31: 1151
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