INTERFACIAL REACTION AND STRENGTHENING MECHANISM OF CERAMIC MATRIX COMPOSITE JOINTS USING LIQUID PHASE DIFFUSION BONDING WITH AUXILIARY PULSE CURRENT

doi:10.11900/0412.1961.2015.00100

Acta Metall Sin

2015, Vol. 51

Issue (9): 1129-1135 DOI: 10.11900/0412.1961.2015.00100

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INTERFACIAL REACTION AND STRENGTHENING MECHANISM OF CERAMIC MATRIX COMPOSITE JOINTS USING LIQUID PHASE DIFFUSION BONDING WITH AUXILIARY PULSE CURRENT

Mingfang WU¹,Fei LIU²,Fengjiang WANG¹(

),Yanxin QIAO¹

1 Key Laboratory of Advanced Welding Technology of Jiangsu Province, Jiangsu University of Science and Technology, Zhenjiang 212003
2 Zhenjiang Institute of Technology, Zhenjiang 212000

Cite this article:

Mingfang WU,Fei LIU,Fengjiang WANG,Yanxin QIAO. INTERFACIAL REACTION AND STRENGTHENING MECHANISM OF CERAMIC MATRIX COMPOSITE JOINTS USING LIQUID PHASE DIFFUSION BONDING WITH AUXILIARY PULSE CURRENT. Acta Metall Sin, 2015, 51(9): 1129-1135.

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Abstract

Ceramic matrix composites (CMCs) is attracted in airspace and nuclear engineering due to their high temperature, corrosion and wearing resistance, but the usage is limited by the joining between CMC and other metals due to obvious incompatibility on physical and chemical aspects on them. The liquid phase-diffusion bonding (LPDB) on Ti(C, N)-Al₂O₃ CMC/Cu joint was studied using the Cu-Zr foil/Cu foil/Cu-Zr foil sanwich as an interlayer in this work. Auxiliary pulse current was also added to control the elemental diffusion and interfacial reaction during LPDB. The element diffusion and reacted products at the interface were analyzed with SEM, EPMA and EDS, and the joint strength was tested with four points bending method. The results show that with an auxiliary pulse current during LPDB, a higher joint strength is reached with a lower bonding temperature and a shorter holding time. The diffusion behavior of element Zr and Cu in CMC and the interfacial area is obviously changed, and the activity of Zr element and its chemical reaction with Al₂O₃ are depressed by the auxiliary pulse current during LPDB. The diffusion of ceramic partilces into the interface and the thickness of corresponding diffusion transition zone (DTZ) and Zr-Cu interfacial reaction zone (IRZ) at the interface are also depressed by the auxiliary pulse current, which strengthens the interface, and is always kept an higher joint strength.

Key words: Ti(C,N)-Al₂O₃ liquid phase diffusion bonding auxiliary pulse current interfacial reaction joint strengthening

Fund: Supported by National Natural Science Foundation of China (No.51175239), Jiangsu Provincial Research Foundation for Basic Research (No.BK2011494) and College Natural Science Foundation of Jiangsu Province (No.11KJA430005)

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https://www.ams.org.cn/EN/10.11900/0412.1961.2015.00100 OR https://www.ams.org.cn/EN/Y2015/V51/I9/1129

Fig.1 Microstructures (a, c) and element distributions by EPMA analysis (b, d) at interface on Ti(C, N)-Al₂O₃ joints bonding at 900 ℃ for 3 min (a, b) and 10 min (c, d) with auxiliary pulse current (The EPMA analysis is scanned along the lines in Figs.1a and c; CMC—ceramic matrix composite, DTZ—diffusion transition zone, IRZ—interfacial reaction zone)

Fig.2 Microstructures (a, c) and element distributions by EPMA analysis (b, d) at interface on Ti(C, N)-Al₂O₃ joints bonding at 980 ℃ for 10 min (a, b) and 30 min (c, d) without auxiliary pulse current

Fig.3 Microstructures (a, c) and element distributions by EPMA analysis (b, d) at interface on Cu/Zr joints bonding at 870 ℃ for 10 min with (a, b) and without (c, d) auxiliary pulse current

Fig.4 Effect of heating temperature and holding time on bending strength of Ti(C, N)-Al₂O₃ joint

Fig.5 Schematic of crack propagation during four points bending testing on Ti(C, N)-Al₂O₃ joint without (a) and with (b) auxiliary pulse current

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