多晶Be室温拉伸变形和断裂行为

  • 许德美 ,
  • 秦高梧 ,
  • 李峰 ,
  • 王战宏 ,
  • 钟景明 ,
  • 李志年 ,
  • 何力军
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  • 1 东北大学材料各向异性与织构教育部重点试验室, 沈阳110819
    2 西北稀有金属材料研究院宁夏特种材料重点实验室, 石嘴山753000
    3 宁夏大学宁夏光伏材料重点实验室, 银川750021
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许德美, 女, 1973年生, 正高职高级工程师, 博士生

修回日期: 2014-02-14

  网络出版日期: 2014-09-25

基金资助

*军品配套科研资助项目JPPT-125-GH-036

TENSILE DEFORMATION AND FRACTURE BEHAVIOR OF POLYCRYSTALLINE BERYLLIUM AT ROOM TEMPERATURE

  • Demei XU ,
  • Gaowu QIN ,
  • Feng LI ,
  • Zhanhong WANG ,
  • Jingming ZHONG ,
  • Zhinian LI ,
  • Lijun HE
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  • 1 Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), Northeastern University, Shenyang 110819
    2 Key Laboratory of Ningxia for Rare Materials, Northwest Rare Metal Materials Research Institute, Shizuishan 753000
    3 Key Laboratory of Ningxia for Photovoltaic Materials, Ningxia University, Yinchuan 750021

Revised date: 2014-02-14

  Online published: 2014-09-25

Supported by

Supported by Auxiliary Program for Military Products (No.JPPT-125-GH-036)

摘要

通过SEM原位拉伸实验观察室温下多晶Be的变形、裂纹萌生和扩展过程, 利用电子背散射衍射(EBSD)标定断裂解理面, 结合OM分析孪晶变形, 研究多晶Be室温拉伸变形和断裂行为及其机理. 结果表明, 室温拉伸应力条件下, 多晶Be的滑移和孪晶变形均难以发生. 滑移带仅在少数取向有利的晶粒中出现, 最终孪晶变形晶粒约占晶粒总数的5%. 变形过程中存在(0001)基面和{1010}柱面之间的交滑移. 多晶Be的微裂纹起源于晶界一侧, 发生穿晶扩展后, 在另一侧晶界终止, 裂纹萌生符合Stroh位错塞积生裂纹理论. 因晶界对裂纹强烈的阻碍作用, 多晶Be的裂纹长大依靠不同微裂纹之间的汇合, 汇合路径有解理台阶和撕裂2种. 多晶Be断裂基本解理面为(0001)基面和{1010}柱面, 两者均是多晶Be解理萌生和扩展的主要路径. 未观察到因孪晶变形诱发的微裂纹.

本文引用格式

许德美 , 秦高梧 , 李峰 , 王战宏 , 钟景明 , 李志年 , 何力军 . 多晶Be室温拉伸变形和断裂行为[J]. 金属学报, 2014 , 50(9) : 1078 -1086 . DOI: 10.11900/0412.1961.2014.00062

Abstract

Deformation and fracture behaviors as well as their mechanisms of polycrystalline beryllium at room temperature were systematically studied by in situ tensile test in SEM, characterizing fracture cleavage planes by electron backscattered diffraction (EBSD) technique, and twinning deformation analyzing by OM. The results show that slip and twinning deformation of polycrystalline beryllium are difficult to occur under tensile stress at room temperature. Slip bands happen only in some grains with a favorable orientation, and finally twinning deformation grain number accounts for only about 5% of the total grains. There exists the cross slip between (0001) basal plane and {1010} prismatic plane in the deformation process. Microcracks usually initiate at one grain boundary, then propagate by a transgranular way and terminate at the other side of the grain boundary in polycrystalline beryllium. Crack initiation of polycrystalline beryllium is in accordance with Stroh dislocation pile-up crack theory. The growth of microcracks have to depend on different microcracks merging by cleavage steps or tearing way due to a strong blocking effect of grain boundaries on the microcracks propagation. Basal cleavage planes of polycrystalline beryllium are determined to be (0001) and {1010} planes. Both of them are the main paths of cleavage crack initiation and propagation of polycrystalline beryllium. It is not observed that twinning deformation induces nucleation of microcracks.

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